This PDF file contains the front matter associated with SPIE Proceedings Volume 9483 including the Title Page, Copyright information, Table of Contents, Introduction, and Conference Committee listing.

In this paper, we have reviewed our research on terahertz (THz) isolators and nonreciprocal transmission devices. In addition, we present a new kind of THz isolator based on asymmetry magneto-metasurface. A structured InSb layer coats on the silica substrate in which the numerical simulation shows that this metasurface has isolation over 60dB at 0.646 THz and a 10dB operating bandwidth of 13 GHz under an external magnetic field of 0.3T with an insertion loss less than 2.5dB. This kind of low-loss, high isolation, easy coupling THz magneto-metasurface isolator has broadly potentials for THz application systems. Importantly, we discuss and conclude the necessary conditions of forming THz nonreciprocal transmission in the magneto-material devices, which is strongly related with magneto-material and asymmetric transmission system.

III-nitride semiconductors having huge longitudinal optical phonon energies are promising as materials to solve a problem of "development of operational frequency range (5-12 THz)" on THz-QCLs. In this study, for the purpose of THz lasing from target subband levels, we designed unique quantum cascade (QC) structures whose active regions consisted of two quantum wells (QWs) for one period and the number of wave-functions contributed to lasing is limited to minimum 3 subband levels. (i.e., Pure 3-level laser system). We fabricated THz-QCLs with QC structures of a pure 3- level laser system (100-200 periods) through a radio-frequency molecular beam epitaxy (RF-MBE) and a metal organic chemical vapor deposition (MOCVD) on MOCVD-growth AlGaN/AlN templates grown on c-plane sapphire substrates. Clear satellite peaks in XRD analyses could be observed, indicating that layer structures were stacked with a good periodicity. By comparing data with simulation spectra, it was found that error of film thicknesses were 1-3 %. We observed sharp lasing spectra with peaks at frequencies of ~5.5 THz and ~7.0 THz whose full width at half maximum (FWHM) values were close to those of resolution of FTIR spectrometer, when we tried pulse current injection measurements into THz-QCL devices. We successfully for the first time realized GaN-based THz-QCL devices lasing at almost the same frequencies as the target ones by designing a 2QWs-type QC structure with a pure 3-level laser system. We also successfully achieved lasing at ~5.5 and ~7.0 THz, which are highest reported to date for any kinds of THz- QCLs.

This paper reviews recent work in the area of active metamaterials where transistors and circuitry are embedded within metamaterial structures for novel functions. In one function, embedding of psuedomorphic high electron mobility transistor (pHEMT) within the metamaterial resonator allows realization of a terahertz modulator. A variation of this approach utilizes diodes to modulate the metamaterial response between a perfect absorber and a perfect detector. In another function, a transistor based power detector is embedded within each metamaterial resonator for roomtemperature detection of gigahertz (GHz) radiation. The realized platform has the potential for high resolution imaging at the diffraction limit. These functions indicate range of novel devices enabled through heterogeneous integration of semiconductor devices with metamaterials.

This paper describes two types of terahertz-wave detector modules implementing a zero-biased InGaAsP Schottky barrier diode (SBD). A SBD was monolithically integrated with a short-stub resonant matching circuit for increasing the detection sensitivity, and assembled in a compact J-band (WR-3) rectangular-waveguide-input module. The module could detect signals at frequencies from 200 to 500 GHz, and its sensitivity peaked at 1460 V/W around 350 GHz, which is a record value for the InP-based zero-biased SBD. A polarization-sensitive sub-terahertz-wave detector was also developed by integrating a SBD and an extended bowtie antenna. The fabricated quasi-optical module could detect signals at frequencies ranging from 30 GHz to 1 THz at zero bias. The principal-polarization-axis angle for signal detection was stable within ±1.5° at frequencies from 80 to 600 GHz, while the degree of polarization was more than 95%.

Recent progress in room-temperature resonant-tunneling-diode (RTD) terahertz (THz) oscillators and high-electron-mobility- transistor (HEMT) THz receivers is reported in this paper. In this study, oscillations up to 1.86 THz were obtained using an optimized antenna and RTD. Using a two-element oscillator array, high output power of 0.6 mW at 620 GHz was obtained. THz communication up to 3 Gbps was demonstrated. A structure for high-speed direct modulation was fabricated, and the intensity modulation up to 30 GHz was achieved. A novel oscillator structure was proposed and fabricated for extraction of output power without using a Si lens. A short-gate InGaAs HEMT detector integrated with a broadband bow-tie antenna was fabricated, and a high current sensitivity of ~5 A/W was obtained at 280 GHz.

Small and fast objects, for example bullets of caliber 5 to 10 mm, fired from guns like AK-47, can cause serious problems to aircrafts in asymmetric warfare. Especially slow and big aircrafts, like heavy transport helicopters are an easy mark of small caliber hand fire weapons. These aircrafts produce so much noise, that the crew is not able to recognize an attack unless serious problems occur and important systems of the aircraft fail. This is just one of many scenarios, where the detection of fast and small objects is desirable. Another scenario is the collision of space debris particles with satellites.

Collaboration between Exelis Geospatial Systems with University of Rochester and Rochester Institute of Technology aims to develop an active THz imaging focal plane array utilizing 0.35um CMOS MOSFET technique. An appropriate antenna is needed to couple incident THz radiation to the detector which is much smaller than the wavelength of interest. This paper simply summarizes our work on modeling the optical characteristics of bowtie antennae to optimize the design for detection of radiation centered on the atmospheric window at 215GHz. The simulations make use of the finite difference time domain method, calculating the transmission/absorption responses of the antenna-coupled detector.

Electromagnetic metamaterials (MMs) consisting of highly conducting sub-wavelength metallic resonators enable many unusual electromagnetic properties at designed frequencies which are not permissible with the naturally occurring materials. The electromagnetic properties of metamaterial are typically controlled by the clever design of the MM unit cell, often termed as meta-molecule, consisting of metallic split ring resonators (SRRs) or meta-atoms. The near field coupling between meta-atoms plays a vital role in tuning the natural resonances of individual SRR and, therefore, has the ability to modify the far-field radiation properties significantly. It is shown that near field coupling between the meta-atoms could lead to resonance tuning, mode splitting, and ultrafast switching in passive and active resonators. In this article, we present a brief review on tuning the metamaterial properties by active and passive manipulation of near field coupling between neighboring split ring resonators.

In this paper the effects of subwavelength antenna resonator element dimensions on the anomalous reflection properties of metasurfaces operating in the millimeter wave and terahertz frequency regions are investigated. Such two-dimensional structures are finding uses as flat optics in a variety of applications including beam steerers, reflectarrays, and broadband, polarization-independent radar absorbers. Numerical simulations were performed to characterize the reflection phase of square resonators of varying dimensions for several metasurface and reflectarray designs. A simple empirical model is developed for efficient characterization of metasurface phase characteristics in lieu of expensive numerical simulation software.

THz radiation is capable of penetrating most of nonmetallic materials and allows THz spectroscopy to be used to image the interior structures and constituent materials of wide variety of objects including Integrated circuits (ICs). The fact that many materials in THz spectral region have unique spectral fingerprints provides an authentication platform to distinguish between authentic and counterfeit electronic components. Counterfeit and authentic ICs are investigated using a high-speed terahertz spectrometer with laser pulse duration of 90 fs and repetition rate of 250 MHz with spectral range up to 3 THz. Time delays, refractive indices and absorption characteristics are extracted to distinguish between authentic and counterfeit parts. Spot measurements are used to develop THz imaging techniques. In this work it was observed that the packaging of counterfeit ICs, compared to their authentic counterparts, are not made from homogeneous materials. Moreover, THz techniques were used to observe different layers of the electronic components to inspect die and lead geometries. Considerable differences between the geometries of the dies/leads of the counterfeit ICs and their authentic counterparts were observed. Observing the different layers made it possible to distinguish blacktopped counterfeit ICs precisely. According to the best knowledge of authors the reported THz inspection techniques in this paper are reported for the first time for authentication of electronic components.

Wide varieties of techniques such as X-ray tomography, scanning electron microscopy (SEM), Energy Dispersive X-ray Spectroscopy (EDS) and optical inspections using a high resolution microscope have also been being employed for detection of counterfeit ICs. In this paper, the achieved data from THz material inspections/ THz imaging are compared to the obtained results from other techniques to show excellent correlation. Compared to other techniques, THz inspection techniques have the privilege to be nondestructive, nonhazardous, less human dependent and fast.

Second-order nonlinear optical wavelength-conversion has been attractive for generating terahertz (THz) wave with high peak-power and for THz-wave detection with high sensitivity. Over 50 kilowatt peak-power THz-wave radiation and sensitive THz-wave detection down to several tens of atto-joule using LiNbO₃ or 4-dimethylamino-N’-methyl-4’- stilbazolium tosylate (DAST) crystals have been demonstrated. LiNbO₃ crystal is an eminent nonlinear crystal for converting wavelengths between THz wave and near infrared (NIR) at frequency range from 1 to 3 THz. Mixing THz wave with an intense NIR pump beam in the LiNbO₃ provides generation of a signal light at a different frequency because of efficient figure of merit. Additionally, sensitivity of up-conversion detection working at room temperature is more than that of cryogenically cooled THz detector. Here, we report on a sensitive THz-wave detection based on novel design using a slant-stripe-type periodically poled Mg doped lithium niobate (PPMgLN) for practical use. The efficient scheme that two optical waves, the pump and up-conversion signal beams, propagate collinearly in the PPMgLN to achieve effective parametric amplification for the signal beam was designed. Minimum THz-wave detection was achieved down to energy about 100 aJ at the frequency of 1.6 THz. The result leads to a novel THz detector based on fiber and integrated optics with high sensitivity, robustness, and easy handling. The nonlinear optical up-conversion detection is promising and broadening THz horizons.

High speed acquisition of reflected terahertz energy constitutes a kinetics spectrum that is an effective tool for layered materials' deformation characterization under ballistic impact. Here we describe utilizing the kinetics spectrum for quantifying a deformation event due to impact in material used for Soldier's helmet. The same technique may be utilized for real-time assessment of trauma by measuring the helmet wore by athletes. The deformation of a laminated material (e.g., a helmet) is dependent on the nature of impact and projectile; thus can uniquely characterize the impact condition leading to a diagnostic procedure based on the energy received by an athlete during an impact. We outline the calibration process for a given material under ballistic impact and then utilize the calibration for extracting physical parameters from the measured kinetics spectrum. Measured kinetics spectra are used to outline the method and rationale for extending the concept to a diagnosis tool. In particular, captured kinetics spectra from multilayered plates subjected to ballistic hit under experimental conditions by high speed digital acquisition system. An algorithm was devised to extract deformation and deformation velocity from which the energy received on the skull was estimated via laws of nonrelativistic motion. This energy is assumed to be related to actual injury conditions, thus forming a basis for determining whether the hit would cause concussion, trauma, or stigma. Such quantification may be used for diagnosing a Soldier’s trauma condition in the field or that of an athlete's.

The terahertz frequency regime is often used as the ‘chemical fingerprint’ region of the electromagnetic spectrum since many molecules exhibit a dense selection of rotational and vibrational transitions. Water is a major component of the atmosphere and since it has a large dipole moment the propagation of terahertz radiation will be dominated by atmospheric effects. This study will present the results of high-­‐resolution broadband measurements of the terahertz atmospheric absorption and detail the technique for directly measuring the pressure broadening coefficients, absolute absorption coefficients, line positions, and continuum effects. Differences between these measured parameters and those tabulated in HITRAN will be discussed. Once the water vapor absorption was characterized, the same technique was used to measure the line parameters for methanol, a trace gas of interest within Earth’s atmosphere. Methanol has a dense absorption spectrum in the terahertz frequency region and is an important molecule in fields such as environmental monitoring, security, and astrophysics. The data obtained in the present study will be of immediate use for the remote sensing community, as it is uncommon to measure this many independent parameters as well as to measure the absolute absorption of the transitions. Current models rely on tabulated databases of calculated values for the line parameters measured in this study. Differences between the measured data and those in the databases will be highlighted and discussed.

We show possibility of the detection and identification of substance at long distance (several metres, for example) using the THz pulse reflected from the object under the real conditions: at room temperature and humidity of about 70%. The main feature of this report consists in a demonstration of the detection and identification of substance using the computer processing of the noisy THz pulse. Amplitude of the useful signal is less than the amplitude of a noise. Nevertheless, it is possible to detect “fingerprint” frequencies of substance if these frequencies are known and the SDA method is used together with new assessments for probability estimation for presence of detected frequencies. Essential restrictions of the commonly used THz TDS method for the detection and identification under real conditions (at long distance about 3.5 m and at a high relative humidity more than 50%) are demonstrated using the physical experiment with chocolate bar and thick paper bag. We show also that the THz TDS method detects spectral features of dangerous substances even in the THz signals measured in laboratory conditions (at distance 30-40 cm from the receiver and at a low relative humidity less than 2%); the n-Si and p-Si semiconductors were used as neutral substances. However, the integral correlation and likeness criteria, based on SDA method, allow us to detect the absence of dangerous substances in the samples. Current results show feasibility of using the discussed method of the THz pulsed spectroscopy for the counter-terrorism problem.

Uncooled microbolometer-type 640x480 and 320x240 Terahertz (THz) focal plane arrays (FPAs) with enhanced sensitivity in sub-THz region are developed, and incorporated into 640x480 and 320x240 cameras, respectively. The pixel in the THz-FPA has such a structure that an area sensitive to electromagnetic wave is suspended above read-out integrated circuit (ROIC). A thin metallic layer is formed on the top of the sensitive area, while a thick metallic layer is formed on the surface of ROIC. The structure composed of the thin metallic layer and the thick metallic layer behaves as an optical cavity. The THz-FPAs reported in this paper have a modified pixel structure which has several times longer optical-cavity length than NEC’s previous pixel does, by forming a thick SiN layer on the ROIC. The extended optical-cavity structure is favorable for detecting electromagnetic wave with lower frequency. Consequently, the Minimum Detectable Power per pixel (MDP) is improved ten times in sub-THz region, especially 0.5-0.6 THz. This paper presents spectral frequency dependences of MDP values for THz-FPA with the modified pixel structure and THz-FPA with the previous pixel structure, using THz free electron laser (FEL) developed by Osaka University. The modification of pixel structure extends high sensitivity region to lower frequency region, such as sub-THz region, and the wider spectral coverage of THz camera surely expands its applicability

False alarm rates must be kept sufficiently low if a method to detect and identify objects or substances is to be implemented in real life applications. This is also true when trying to detect and identify dangerous substances such as explosives and drugs that are concealed in packaging materials. THz technology may be suited to detect these substances, especially when imaging and spectroscopy are combined. To achieve reasonable throughput, the detection and identification process must be automated and this implies reliance on algorithms to perform this task, rather than human beings. The identification part of the algorithm must compare spectral features of the unknown substance with those in a library of features and determining the distance, in some sense, between these features. If the distance is less than some defined threshold a match is declared. In this paper we consider two types of spectral characteristic that are derived from measured time-domain signals measured in the THz regime: the absorbance and its derivative. Also, we consider two schemes to measure the distance between the unknown and library characteristics: Spectral Angle Mapping (SAM) and Principal Component Analysis (PCA). Finally, the effect of windowing of the measured time-domain signal on the performance of the algorithms is studied, by varying the Blackman-Harris (B-H) window width. Algorithm performance is quantified by studying the receiver-operating characteristics (ROC). For the data considered in this study we conclude that the best performance is obtained when the derivative of the absorbance is used in combination with a narrow B-H window and SAM. SAM is a more straight-forward method and requires no large training data sets and tweaking.

Exelis Geospatial Systems and its CEIS partners at the University of Rochester and Rochester Institute of Technology are developing an active THz imaging system for use in standoff detection, molecular spectroscopy and penetration imaging. The current activity is focused on developing a precision instrument for the detection of radiation centered on atmospheric windows between 200 GHz and 400 GHz (available sources). A transmission imager is developed by raster scanning through a semi-coherent non-ionizing beam, where the beam is incident on a NMOS FET detector. The primary goal of the initial system is to produce a setup capable of measuring responsivity and sensitivity of the detector. The Instrumentation covers the electromagnetic spectral range between 188 GHz and 7.0 THz. Transmission measurements are collected at 188 GHz in order to verify image formation, responsivity and sensitivity as well as demonstrate the active imager’s ability to make penetration images.

Development of infrared and sub-terahertz radiation detectors at the same sensitive elements on the base of mercurycadmium- telluride (MCT) is reported. Two-color un-cooled and cooled to 78 K narrow-gap MCT semiconductor thin layers, grown by liquid phase epitaxy or molecular beam epitaxy method on high resistivity CdZnTe or GaAs substrates, with bow-type antennas were considered both as sub-terahertz direct detection bolometers and 3 to 10 μm infrared photoconductors. Their room temperature noise equivalent power (NEP) at frequency ~ 140 GHz and signal-to-noise ratio (S/N) in the spectral sensitivity maximum under the monochromatic (spectral resolution of ~0.1 μm) globar illumination were reached NEP ~4.5*10^-10 W/Hz^1/2 and S/N~50, respectively.

Two different THz applications in the semiconductor industry were explored and validated against established reference measurement techniques and simulations. The first application investigated the possibility of measuring mechanical deformation behaviour of silicon wafers. Time-domain THz tomography mapping scans were carried out to measure wafer thickness and flatness, both in the native state and under different external mechanical loads. These measurements were carried out for a variety of wafers, and the ensuing deformation maps used to validate newly developed numerical simulation models for wafer deformation, and vice versa. In the second part of this paper, carrier dynamics of optically injected charges were investigated by THz spectroscopy. THz pump/probe measurements were carried out in transmission and reflection arrangements on silicon wafers illuminated by a metal halide light source. The light source generates free charge carriers in the semiconductor material that affect the transmission and reflection properties of the semiconductor material. The results of the THz measurements are compared to established standard techniques, like microwave-detected photo-conductance decay (MWPCD) or quasi-steady-state photo conductance (QSSPC) measurements. The defective areas identified with the THz measurements are in good agreement with the defective areas identified by the reference methods. A common benefit of time-domain THz measurements is that the wafer thickness, which is an important measure for the interaction volume of the THz radiation with the semiconductor material, can be calculated from the time- domain signals. The results indicate that THz spectroscopy and imaging can be valuable tools for defect analysis and quality control of silicon wafers, especially since the measurement is fully contact-free and can determine mechanical and electrical properties within a single modality.

A relatively high Mg mole fraction of 7% is achieved using the cavitation effect under sonication to overcome the low solubility of ZnO-MgO at low temperature. The Mg mole fraction is confirmed by shift in the near band emission of free exciton under photoluminescence spectroscopy at room temperature. The x-ray diffraction pattern has a large peak associated to ZnO (002) from which the c-lattice constant is calculated to be 5.1967Ǻ. The nanorods (NRs) grown via sonochemical are compared to nanowires (NWs) grown using metal organic chemical vapor deposition (MOCVD) and hydrothermal synthesis. Also, the effect of the ZnO film used as seed layer is described and compare to a simple spin coated layer. Terahertz (THz) index of refraction and dielectric constant of wurtzite Zn_1-xMg_xO NWs with Mg mole fraction of 7% via sonochemical are determined using THz time domain spectroscopy (THz-TDS). The results are compared with ZnO and ZnMgO NWs with 10% Mg mole fraction grown using MOCVD. The successful growth of Zn_1-xMg_xO with wurtzite structure at low temperature permits realization of the growth of heterostructures, quantum well, nanowires and nanorods on flexible substrates providing lower cost, optical and carrier confinement necessary in advanced light emitting diodes (LEDs), laser diodes (LDs) and high efficiency solar cells.