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17 February 1997 Field ion spectrometry: a new technology for cocaine and heroin detection
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Proceedings Volume 2937, Chemistry- and Biology-Based Technologies for Contraband Detection; (1997) https://doi.org/10.1117/12.266764
Event: Enabling Technologies for Law Enforcement and Security, 1996, Boston, MA, United States
Abstract
Field ion spectrometry, also known as transverse field compensation ion mobility spectrometry, is a new technique for trace gas analysis that can be applied to the detection of cocaine and heroin. Its principle is based on filtering ion species according to the functional dependence of their mobilities with electric field strength. Field ion spectrometry eliminates the gating electrodes needed in conventional IMS to pulse ions into the spectrometer; instead, ions are injected in to the spectrometer and reach the detector continuously, resulting in improved sensitivity. The technique enables analyses that are difficult with conventional constant field strength ion mobility spectrometers. We have shown that a filed ion spectrometer can selectively detect the vapors from cocaine and heroin emitted from both their base and hydrochloride forms. The estimated volumetric limits of detection are in the low pptv range, based on testing with standardized drug vapor generation systems. The spectrometer can detect cocaine base in the vapor phase, at concentrations well below its estimated 100 pptv vapor pressure equivalent at 20 degrees C. This paper describes the underlying principles of field ion spectrometry in relation to narcotic drug detection, and recent results obtained for cocaine and heroin. The work has been sponsored in part by the United States Advanced Research Projects Agency under contract DAAB10-95C-0004, for the DOD Counterdrug Technology Development Program.
© (1997) COPYRIGHT Society of Photo-Optical Instrumentation Engineers (SPIE). Downloading of the abstract is permitted for personal use only.
Byron L. Carnahan, Stephen Day, Viktor Kouznetsov, and Alexandre Tarassov "Field ion spectrometry: a new technology for cocaine and heroin detection", Proc. SPIE 2937, Chemistry- and Biology-Based Technologies for Contraband Detection, (17 February 1997); https://doi.org/10.1117/12.266764
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