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In this paper the method of structural and optical properties of novel crystals of the [N(C3H7)4]2MeBr4 (Me = Zn, Co, Cu)
will be presented. The X-ray investigations were carried out using four-circle diffractometer KM4-CCD at room
temperature Optical spectra of samples were measured using AVS-S2000 and 1725 FI -IR spectrometers. Connections
between optical properties of the studied crystals and electronic configuration of transition metal ions will be considered.
An influence of metal ion substitution on the shape of the optical spectra of crystals will be also discussed.
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