15 October 2019 Development of large-size multilayer mirrors with a linear deposition facility for x-ray applications
Hangjian Ni, Qiushi Huang, Yingna Shi, Runze Qi, Zhe Zhang, Yufei Feng, Xudong Xu, Zhong Zhang, Jie Wang, Zhongliang Li, Lian Xue, Ling Zhang, Zhanshan Wang
Author Affiliations +
Abstract

Driven by the growing demand for large-size x-ray mirrors used in synchrotron radiation and free-electron laser facilities, a linear deposition system based on magnetron sputtering technique is built. The layer growth quality and thickness uniformity are optimized by adding masks in front of the cathode to reduce the oblique-incidence particles and tune the sputtering flux distribution. Based on this, a 0.5-m-length W/Si multilayer mirror is demonstrated. The multilayer has a d-spacing of 3 nm and a bilayer number of 60. The surface roughness of the multilayer is only 0.33 to 0.25 nm in the spatial frequency range of 3.0  ×  10  −  3 to 1.0  μm  −  1, and the average interface width is 0.32 nm. The hard x-ray reflectivity and uniformity of the large mirror were characterized at the Optics Beamline in Shanghai Synchrotron Radiation Facility. A maximum reflectivity of 62.5% and 62.7% was measured at 8 and 18 keV, respectively, with an angular resolution of Δθ  /  θ  =  2.7  %  . The d-spacing uniformity over the 0.5-m-length and 60-mm-width area of the mirror is 1.0% and 1.2% (peak-to-valley), respectively. These results indicate a good and uniform quality of the nanoscale multilayer over the large mirror area. The measured second- and third-order reflectivities of the multilayer are more than 2 orders magnitude lower than the first order, implying a good suppression of high harmonics in the monochromator application.

© 2019 Society of Photo-Optical Instrumentation Engineers (SPIE) 0091-3286/2019/$28.00 © 2019 SPIE
Hangjian Ni, Qiushi Huang, Yingna Shi, Runze Qi, Zhe Zhang, Yufei Feng, Xudong Xu, Zhong Zhang, Jie Wang, Zhongliang Li, Lian Xue, Ling Zhang, and Zhanshan Wang "Development of large-size multilayer mirrors with a linear deposition facility for x-ray applications," Optical Engineering 58(10), 104105 (15 October 2019). https://doi.org/10.1117/1.OE.58.10.104105
Received: 20 July 2019; Accepted: 25 September 2019; Published: 15 October 2019
Lens.org Logo
CITATIONS
Cited by 5 scholarly publications.
Advertisement
Advertisement
RIGHTS & PERMISSIONS
Get copyright permission  Get copyright permission on Copyright Marketplace
KEYWORDS
Mirrors

Reflectivity

Multilayers

X-rays

Sputter deposition

Interfaces

Silicon

RELATED CONTENT

Small-d-spacing WSi2/Si narrow bandpass multilayers
Proceedings of SPIE (November 03 2004)
Multilayer mirrors for XUV Ge laser wavelengths
Proceedings of SPIE (January 01 1992)
Multi-layer coating development for XEUS
Proceedings of SPIE (June 13 2006)
Multilayers for next-generation x-ray sources
Proceedings of SPIE (May 18 2007)

Back to Top