The outgassing characteristic of the silicone rubber which is the main material of non-metallic materials in high power laser system was studied,outgassing rates of the silicone rubber and the baked-out silicone rubber which was performed at 80°C4 hours were measured by the constant volume process method,and outgassing properties of them were analyzed by the quadrupole mass spectrometer. The results show that the outgassing rate of the silicone rubber and the baked-out silicone rubber is 2.69×10-7 Pa·m3s-1cm-2 and 6.47×10-8 Pa·m3s-1cm-2 , respectively. All of them give out condensable volatile matter in vacuum. The outgassing rate and condensable volatile matter of the baked-out silicone rubber are less an order of magnitude compared with the silicone rubber, and the outgassing rate of the silicone rubber is less than 1×10-7 Pa·m3s-1cm-2, which is fit for non-metallic material of the high power laser system. This paper also discusses the method of reducing the outgassing rate and condensable volatile matter of the silicone rubber in high power laser system.
Measuring penetration rates of water vapor and oxygen though OLED packaging materials by mass spectrometry is a new method. Currently, the sampling of penetration gas is dynamic sampling method. The sensitivity of this method is magnitude of 10-4 g/m2day, which can not reach the ideal magnitude of 10-6 g/m2day. Static accumulation sampling method for improving sensitivity of measuring is present in this paper. Comparing with dynamic sampling method, the sensitivity of this sampling method has been improved 1-2 magnitudes. The devices of static accumulation sampling method have been designed. The experiments of measuring penetration rates of water vapor and oxygen through packaging materials have been done. The results and analysis of the experiments have been introduced.
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