The Auroral x-ray Imaging Spectrometer (AXIS) instrument proposed by the Indian Space Research Organisation’s (ISRO) Space Astronomy Group plans to gather spectral information of the Earth’s aurorae in the 0.3 to 3keV band from a low Earth polar orbit for the first time. A trade-off study comparing possible Teledyne e2v (Te2v) detectors to meet preliminary instrument requirements previously concluded that the backside-illuminated (BI) CIS221-X, a prototype CMOS image sensor (CIS) optimised for soft x-ray detection, was a viable option. This paper introduces the current preliminary instrument requirements for AXIS and the compact Nuscis camera electronics from XCAM Ltd that will be used with the CIS221-X to produce an engineering model of the instrument. Continued studies on the CIS221-X for AXIS will include the optimisation of operating conditions in particular for the less well-studied pixel variants of the detector, and calibration with soft x-rays.
As space agencies consider the next generation of large space telescopes, it is becoming clear that high performance Ultraviolet (UV) imaging will be a key requirement. High-performing CMOS image sensors that are optimised for UV detection performance will therefore be essential for these missions to be able to fulfil their science requirements. The CASTOR mission, a 1m UV space telescope project, will be utilising the large format CIS303 and CIS120 detectors from Teledyne e2v for three large focal planes covering the UV , u ′ and g ′ bands, respectively. Typically, silicon sensors have a very low quantum efficiency (QE) in the UV band between 150- 300 nm, and the 2d-doping technology from NASA/JPL will therefore be utilised to improve the quantum efficiency. The Open University will perform electro-optical testing and space qualification of the CIS303 and CIS120 detectors, including a comparison of different UV coating and enhancement technologies. This paper covers the specification of radiation testing of the CIS303 and CIS120 detectors at the Open University, and characterisation of the QE-enhancing surface treatments.
Energy-dispersive imaging spectroscopy of X-ray emission from the Earth’s aurorae promises to further knowledge in the field of aeronomy. Time- and spatially-resolved observations of fluorescence from the dominant atmospheric components require the detection of X-rays as soft as 390 eV with a resolution of no more than 100 eV at these energies. The Auroral X-ray Imaging Spectrometer (AXIS) instrument of the Disturbed and quiet time Ionosphere-thermosphere System at High Altitudes (DISHA) mission is expected to perform these observations.
The baseline instrument design has suggested the use of an electron-multiplying charge-coupled device (EMCCD). The EMCCD’s electron-multiplying register can reduce the effective readout noise and enable the detection of signals as small as a single photoelectron. For the detection of soft X-rays, however, the noise penalty from the EM register’s stochastic process degrades energy resolution.
Emerging CMOS image sensors (CIS), particularly the Teledyne e2v CIS221-X test device, with back illumination, full depletion (with 36 μm thickness), large pixel sizes (40 μm), and low readout noise (3 e- rms effective) are expected to achieve the required performance without the effects of the EM register. Simple models for X-ray event sensitivity, detectability, and resolution, indicate that candidate CIS equal or better EMCCD performance. Furthermore, CIS offer other advantages including lower power consumption, higher operating temperature, and increased radiation hardness. However, these sensors introduce other behaviors that may impact their apparent benefits, which initial experimental testing and analyses are working to understand.
An optical bench setup for quantum efficiency (QE) measurements across the 350 nm to 1100 nm range has been developed at the Open University’s Centre for Electronic Imaging (CEI). Here we use it to measure the performance of a monolithic silicon CMOS image sensor (CIS), the CIS115. This sensor was selected for the JANUS camera, due to launch on board ESA’s JUpiter ICy moons Explorer (JUICE) spacecraft in 2022. The CIS115 sensors tested here have high quantum efficiency (QE) over the optical band, due to their backside illumination and multi-layer anti-reflective coating. Here we validate the QE measurements against manufacturer reported performance and compare the QE for unirradiated (beginning of life) and gamma-irradiated devices, indicating that no significant change in performance should be expected after a total ionizing dose (TID) of 200 krad(Si). This is important for the JANUS application, where the sensor is predicted to accumulate up to 44 krad(Si) TID. We also demonstrate that the measurement setup has excellent repeatability. We conclude by discussing the limitations of the setup, including the key systematic error sources that have been understood and investigated. Optional improvement to the setup for reducing these errors are presented and will be considered for follow-on activities.
Teledyne-e2v’s sensors and wafer-scale processing are widely used for high performance imaging across soft X-ray and optical bands. In the ultraviolet spectral range, the combination of short absorption lengths (below 10 nm) and high reflectance (up to 75 %) can strongly limit the quantum efficiency. Direct detection capability relies on back-illumination and back-thinning processes to be applied to a sensor to remove dead layers from the optical path. As the thinning process leaves an unacceptably thick backside potential well as well as a highly reflective surface, in-house ultraviolet-specific (e.g. for WUVS) or third-party processes (e.g. delta-doping for FIREBall) are required. We have calibrated Teledyne-e2v’s latest in-house wafer-scale proprietary processes with monochromatic synchrotron radiation over a wide spectral range in the ultraviolet domain (λ=40 nm – 400 nm) at the Metrology Light Source of the Physikalisch-Technische Bundesanstalt. The first process is a shallow p+ implantation that permits the thinning of the backside potential well. It is available in two different levels: basic and enhanced. The second type of enhancement is a specific anti-reflective coating to increase the back-surface transmittance for distinct spectral ranges. In this paper, we will present comparative quantum efficiency calibration of both passivation stages and of two different ultraviolet specific anti-reflective coatings (applied on enhanced passivation devices). Also, their stability after intense ultraviolet illumination will be shown. These measurements will permit Teledyne-e2v to extend the quantum efficiency data of their most recent processes across the soft X-ray to near-infrared spectrum.
X-ray backscatter (XBS) provides a novel approach to the field of non-destructive evaluation (NDE) in the aerospace industry. XBS is conducted by collecting the radiation which is scattered from a sample illuminated by a well-defined Xray beam, and the technique enables objects to be scanned at a sub-surface level using single-sided access, and without the requirement for coupling with the sample. Single-sided access is of particular importance when the objects of interest are very large, such as aircraft components. Carbon fibre composite materials are being increasingly used as a structural material in aircraft, and there is an increasing demand for techniques which are sensitive to the delaminations which occur in these composites as a result of both large impacts and barely visible impact damage (BVID). The XBS signal is greatly enhanced for plastics and lightweight materials, making it an ideal candidate for probing sub-surface damage and defects in carbon fibre composites. Here we present both computer modelling and experimental data which demonstrate the capability of the XBS technique for identifying hidden defects in carbon fibre.
The prevalence of counterfeit and substandard medicines has been growing rapidly over the past decade, and fast, nondestructive techniques for their detection are urgently needed to counter this trend. In this study, energy-dispersive X-ray diffraction (EDXRD) combined with chemometrics was assessed for its effectiveness in quantitative analysis of compressed powder mixtures. Although EDXRD produces lower-resolution diffraction patterns than angular-dispersive X-ray diffraction (ADXRD), it is of interest for this application as it carries the advantage of allowing the analysis of tablets within their packaging, due to the higher energy X-rays used. A series of caffeine, paracetamol and microcrystalline cellulose mixtures were prepared with compositions between 0 - 100 weight% in 20 weight% steps (22 samples in total, including a centroid mixture), and were pressed into tablets. EDXRD spectra were collected in triplicate, and a principal component analysis (PCA) separated these into their correct positions in the ternary mixture design. A partial least-squares (PLS) regression model calibrated using this training set was validated using both segmented cross-validation, and with a test set of six samples (mixtures in 8:1:1 and 5⅓:2⅓:2⅓ ratios) – the latter giving a root-mean square error of prediction (RMSEP) of 1.30, 2.25 and 2.03 weight% for caffeine, paracetamol and cellulose respectively. These initial results are promising, with RMSEP values on a par with those reported in the ADXRD literature.
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